| Name | 1,10-Dibromodecane |
| Synonyms | Dibromodecane 1,10-DIBROMODECANE 1,10-Dibromodecane TIMTEC-BB SBB008900 1,10-DECANE DIBROMIDE DECAMETHYLENE BROMIDE DECAMETHYLENE DIBROMIDE Decamethylene dibromide 1,10-DECAMETHYLENE BROMIDE 1,10-DECAMETHYLENE DIBROMIDE |
| CAS | 4101-68-2 |
| EINECS | 223-871-0 |
| InChI | InChI=1/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2 |
| InChIKey | GTQHJCOHNAFHRE-UHFFFAOYSA-N |
| Molecular Formula | C10H20Br2 |
| Molar Mass | 300.07 |
| Density | 1.335 g/mL at 25 °C (lit.) |
| Melting Point | 25-27 °C (lit.) |
| Boling Point | 160 °C/15 mmHg (lit.) |
| Flash Point | 26°C |
| Water Solubility | insoluble |
| Vapor Presure | 0.00233mmHg at 25°C |
| Appearance | White crystal |
| Specific Gravity | 1.335 |
| Color | Beige to brown |
| BRN | 506156 |
| Storage Condition | Sealed in dry,Room Temperature |
| Sensitive | Easily absorbing moisture |
| Refractive Index | n20/D 1.4912(lit.) |
| MDL | MFCD00000222 |
| Physical and Chemical Properties | White flaky crystals. Melting point 27 ℃(25.5-26 ℃), boiling point 161-162.4 ℃(1.2kPa),110 ℃(4 × 10-2kPa), relative density 1.335(30/4 ℃), refractive index 1.4905(30 degrees C). Soluble in ethanol, slightly soluble in cold ethanol, insoluble in water. Deliquescence. |
| Use | Used as an intermediate in organic synthesis. |
| Risk Codes | R20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. R36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S22 - Do not breathe dust. S24/25 - Avoid contact with skin and eyes. S36 - Wear suitable protective clothing. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. |
| WGK Germany | 3 |
| TSCA | Yes |
| HS Code | 29049090 |
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| Use | Used as an intermediate in organic synthesis. |
| Production method | It is obtained by the reaction of decanediol and hydrogen bromide. Heat decanediol to 95-100°C, and pass in dry hydrogen bromide gas under stirring. When the hydrogen bromide in the mixture is saturated, the temperature is raised to 135 ℃, and hydrogen bromide is slowly introduced. Cooling, dividing the water layer to obtain the coarse product. Wash with water, then wash with 10% sodium carbonate solution, remove all the acid and then carry out reduced pressure distillation, collect 139-142 ℃(0.266kPa) fraction to obtain the finished product. |